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The monograph presents research results on the study of the synthesis process of organohybrid sorbents containing nitrogen, sulfur, and silicon, their physicochemical properties, as well as the possibilities and technology of the field of application, as well as the modern interpretation of the production of new types of organohybrid sorbents, the synthesis of several types of organ hybrid sorbents and analytical and research materials consisting of 4 chapters are presented, including research methods, their discussion, and the technological scheme of obtaining these sorbents. This book is recommended as a guide for senior students of chemical technology of organic and inorganic substances of technological higher education institutions. It is especially recommended as a guide for specialists engaged in organic and inorganic synthesis, researchers researching the sorption of rare and rare metals, and purification of wastewater from heavy metals.