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This book represents the crystal growth of Germanium Selenide doped by Pb single crystals, and these single crystals were thermally characterized. Further, another synthesis has been represented of Tin Selenide nanoparticles doped by Cu. Thus, thermal characterization of Single crystal semiconductors as well as nanoparticles has been covered fully in this book. A brief explanation of the results covered in the book as content of the different chapters.