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This book is useful for pharmacy post graduate students and research scholars who wish to pursue their research in the field of pharmaceutical analysis. In this book, Chapter 1 deals with the aim, objective and general introduction regarding analytical method development, optimization and validation. Chapter 2 deals with the literature survey of the selected drugs namely Cefpirome Sulphate, Aceclofenac and Diacerin. Chapter 3 deals with the HPLC methods developed for Cefpirome Sulphate, Aceclofenac and Diacerin. Chapter 4 deals with UV methods developed for these drugs. Chapter 5 deals with the summery and conclusion. References are included at the end.