Editors Vladimir K. Michaelis is Assistant Professor in the Department of Chemistry at the University of Alberta. Robert G. Griffin is Professor of Chemistry and Director of the Francis Bitter Magnet Laboratory at the Massachusetts Institute of Technology. Björn Corzilius is Professor of Physical Chemistry in the Institute of Chemistry at the University of Rostock. Shimon Vega is Professor in the Department of Chemical Physics at the Weizmann Institute of Science, Israel.
Inhaltsangabe
Contributors xi Series Preface xvii Preface xix Acknowledgments xxi Part A: Concepts, Theory, & Instrumentation 1 1 The Discovery and Demonstration of Dynamic Nuclear Polarization-A Personal and Historical Account 3 Charles P. Slichter 2 DNP Mechanisms 15 Krishnendu Kundu, Frédéric Mentink-Vigier, Akiva Feintuch, and Shimon Vega 3 Pulsed Dynamic Nuclear Polarization 71 Kong Ooi Tan, Sudheer Jawla, Richard J. Temkin, and Robert G. Griffin 4 MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity 87 Sabine Hediger, Daniel Lee, Frédéric Mentink-Vigier, and Gaël De Paëpe 5 Polarizing Agents: Evolution and Outlook in Free Radical Development for DNP 103 Gilles Casano, Hakim Karoui, and Olivier Ouari 6 Paramagnetic Metal Ions for Dynamic Nuclear Polarization 121 Björn Corzilius 7 Instrumentation for High-field Dynamic Nuclear Polarization NMR Spectroscopy 143 Guy M. Bernard and Vladimir K. Michaelis 8 Millimeter-wave Sources for DNP-NMR 155 Monica Blank and Kevin L. Felch 9 Cryogenic Platforms and Optimized DNP Sensitivity 169 Yoh Matsuki and Toshimichi Fujiwara 10 Versatile Dynamic Nuclear Polarization Hardware with Integrated Electron Paramagnetic Resonance Capabilities 189 Alisa Leavesley, Ilia Kaminker, and Songi Han 11 Dissolution Dynamic Nuclear Polarization Methodology and Instrumentation 219 Dennis Kurzbach and Sami Jannin 12 Introduction to Dissolution DNP: Overview, Instrumentation, and Human Applications 239 Jan H. Ardenkjaer-Larsen 13 Liquid-state Overhauser DNP at High Magnetic Fields 261 Vasyl P. Denysenkov and Thomas F. Prisner 14 Overhauser DNP in Liquids on 13C Nuclei 279 Marina Bennati and Tomas Orlando Part B: Applications 289 15 DNP and Cellular Solid-state NMR 291 Alessandra Lucini Paioni, Marie A.M. Renault, and Marc Baldus 16 Cryo-trapped Intermediates of Retinal Proteins Studied by DNP-enhanced MAS NMR Spectroscopy 305 Johanna Becker-Baldus and Clemens Glaubitz 17 DNP Solid-state NMR of Biological Membranes 323 Burkhard Bechinger 18 DNP in Materials Science: Touching the Surface 337 Pierrick Berruyer, Lyndon Emsley, and Anne Lesage 19 Growing Signals from the Noise: Challenging Nuclei in Materials DNP 353 Frédéric A. Perras, Takeshi Kobayashi, and Marek Pruski 20 DNP-enhanced Solid-state NMR Spectroscopy of Active Pharmaceutical Ingredients 373 Li Zhao, Arthur C. Pinon, Lyndon Emsley, and Aaron J. Rossini 21 In Vivo Hyperpolarized 13C MRS and MRI Applications 405 Irene Marco-Rius and Arnaud Comment 22 Dissolution Dynamic Nuclear Polarization 421 Walter Köckenberger Index 435
Contributors xi Series Preface xvii Preface xix Acknowledgments xxi Part A: Concepts, Theory, & Instrumentation 1 1 The Discovery and Demonstration of Dynamic Nuclear Polarization-A Personal and Historical Account 3 Charles P. Slichter 2 DNP Mechanisms 15 Krishnendu Kundu, Frédéric Mentink-Vigier, Akiva Feintuch, and Shimon Vega 3 Pulsed Dynamic Nuclear Polarization 71 Kong Ooi Tan, Sudheer Jawla, Richard J. Temkin, and Robert G. Griffin 4 MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity 87 Sabine Hediger, Daniel Lee, Frédéric Mentink-Vigier, and Gaël De Paëpe 5 Polarizing Agents: Evolution and Outlook in Free Radical Development for DNP 103 Gilles Casano, Hakim Karoui, and Olivier Ouari 6 Paramagnetic Metal Ions for Dynamic Nuclear Polarization 121 Björn Corzilius 7 Instrumentation for High-field Dynamic Nuclear Polarization NMR Spectroscopy 143 Guy M. Bernard and Vladimir K. Michaelis 8 Millimeter-wave Sources for DNP-NMR 155 Monica Blank and Kevin L. Felch 9 Cryogenic Platforms and Optimized DNP Sensitivity 169 Yoh Matsuki and Toshimichi Fujiwara 10 Versatile Dynamic Nuclear Polarization Hardware with Integrated Electron Paramagnetic Resonance Capabilities 189 Alisa Leavesley, Ilia Kaminker, and Songi Han 11 Dissolution Dynamic Nuclear Polarization Methodology and Instrumentation 219 Dennis Kurzbach and Sami Jannin 12 Introduction to Dissolution DNP: Overview, Instrumentation, and Human Applications 239 Jan H. Ardenkjaer-Larsen 13 Liquid-state Overhauser DNP at High Magnetic Fields 261 Vasyl P. Denysenkov and Thomas F. Prisner 14 Overhauser DNP in Liquids on 13C Nuclei 279 Marina Bennati and Tomas Orlando Part B: Applications 289 15 DNP and Cellular Solid-state NMR 291 Alessandra Lucini Paioni, Marie A.M. Renault, and Marc Baldus 16 Cryo-trapped Intermediates of Retinal Proteins Studied by DNP-enhanced MAS NMR Spectroscopy 305 Johanna Becker-Baldus and Clemens Glaubitz 17 DNP Solid-state NMR of Biological Membranes 323 Burkhard Bechinger 18 DNP in Materials Science: Touching the Surface 337 Pierrick Berruyer, Lyndon Emsley, and Anne Lesage 19 Growing Signals from the Noise: Challenging Nuclei in Materials DNP 353 Frédéric A. Perras, Takeshi Kobayashi, and Marek Pruski 20 DNP-enhanced Solid-state NMR Spectroscopy of Active Pharmaceutical Ingredients 373 Li Zhao, Arthur C. Pinon, Lyndon Emsley, and Aaron J. Rossini 21 In Vivo Hyperpolarized 13C MRS and MRI Applications 405 Irene Marco-Rius and Arnaud Comment 22 Dissolution Dynamic Nuclear Polarization 421 Walter Köckenberger Index 435
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