In an era where the global demand for sustainable and high-performance energy storage devices continues to grow, this comprehensive work presents an in-depth investigation into the design, synthesis, and electrochemical evaluation of advanced nanocomposite electrodes for supercapacitor applications. Through careful experimentation and innovative material engineering, the book explores the development of pristine and hybrid nanostructured materials based on cobalt oxide (Co O ), reduced graphene oxide (rGO), and polyaniline (PANI), highlighting how structural engineering and interfacial compatibility among inorganic, carbonaceous, and conducting polymer components contribute to enhanced charge storage behavior. The book provides a comprehensive introduction to energy storage systems, discussing their charge storage mechanisms, performance metrics, and material requirements. It includes a detailed literature review of recent advancements in supercapacitor materials and identifies key research gaps that motivate the present work. It demonstrates the powerful synergistic methods, validating the potential of hybrid electrodes for advancing energy storage technology.
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