This practical guide shows how to efficiently use the method for a variety of applications. Numerous examples as well as ideas for problem solving and troubleshooting are presented. The new edition is updated with the latest developments in methods and applications.
This practical guide shows how to efficiently use the method for a variety of applications. Numerous examples as well as ideas for problem solving and troubleshooting are presented. The new edition is updated with the latest developments in methods and applications.
Joachim Nölte studied and completed his PhD degree in environmental analysis at the University of Hamburg, Germany. His work has focussed on ICP OES since 1981 and he has worked at Perkin Elmer on method development. He has extensive experience in teaching the method through courses and presentations. In 2000 he founded a consulting agency called AnalytikSupport.
Inhaltsangabe
OVERVIEW Analytic features of the ICP OES ICP OES - definitions Distribution of the ICP emission spectrometers Complimentary techniques for elemental analysis MIP and LIPS Symbols, abbreviations and acronyms used
PLASMA The analytically used plasma Argon Added gases (e.g. Oxygen or Nitrogen) Materials used for ICP torches Orientation of the plasma (e.g. vertical vs. horizontal) Excitation to emit electromagnetic radiation High-frequency generator Sample introduction system Nebulizers
OPTICS AND DETECTOR OF THE SPECTROMETER Principles of optics Detector Emission spectrometer mounts Scanning Array Spectrometers Simultaneous Array Spectrometers
METHOD DEVELOPMENT Wavelength selection Reference to NIST-Atlas Processing and correction techniques Non-spectral interferences Optimization Validation Procedure to check linearity
ROUTINE ANALYSIS Preliminary steps Calibration Quality control Software and data management
TROUBLE SHOOTING
APPLICATIONS General Notes Notes on specific elements Selected applications
INSTRUMENT PURCHASING AND LABORATORY PREPARATION Which technique in atomic spectrometry is preferred? Which ICP emission spectrometer is best for the application? Preparation of the laboratory
OVERVIEW Analytic features of the ICP OES ICP OES - definitions Distribution of the ICP emission spectrometers Complimentary techniques for elemental analysis MIP and LIPS Symbols, abbreviations and acronyms used
PLASMA The analytically used plasma Argon Added gases (e.g. Oxygen or Nitrogen) Materials used for ICP torches Orientation of the plasma (e.g. vertical vs. horizontal) Excitation to emit electromagnetic radiation High-frequency generator Sample introduction system Nebulizers
OPTICS AND DETECTOR OF THE SPECTROMETER Principles of optics Detector Emission spectrometer mounts Scanning Array Spectrometers Simultaneous Array Spectrometers
METHOD DEVELOPMENT Wavelength selection Reference to NIST-Atlas Processing and correction techniques Non-spectral interferences Optimization Validation Procedure to check linearity
ROUTINE ANALYSIS Preliminary steps Calibration Quality control Software and data management
TROUBLE SHOOTING
APPLICATIONS General Notes Notes on specific elements Selected applications
INSTRUMENT PURCHASING AND LABORATORY PREPARATION Which technique in atomic spectrometry is preferred? Which ICP emission spectrometer is best for the application? Preparation of the laboratory
LITERATURE INDEX
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