Introduction to Organic Laboratory Techniques

A Microscale Approach
By Donald L. Pavia, Gary M. Lampman, George S. Kriz et al.

• Gebundenes Buch

Produktdetails

• Brooks / Cole Laboratory Series for Organic Chemistry
• Verlag: Cengage Learning EMEA
• 4th ed., Int. Stud. Ed.
• Seitenzahl: 990
• Englisch
• Abmessung: 285mm
• Gewicht: 2058g
• ISBN-13: 9780495388876
• ISBN-10: 0495388874
• Artikelnr.: 22926042

Inhaltsangabe

Part One: INTRODUCTION TO BASIC LABORATORY TECHNIQUES.Experiment 1: Introduction to Microscale Laboratory.Experiment 2: Solubility.Experiment 3: Crystallization.Experiment 4: Extraction.Experiment 5: Chromatography.Experiment 6: Simple and Fractional Distillation.Experiment 6A: Simple and Fractional Distillation (Semi-Microscale Procedure).Experiment 6B: Simple and Fractional Distillation (Microscale Procedure).Experiment 7: Infrared Spectroscopy and Boiling-Point Elevation.Essay Aspirin.Experiment 8: Acetylsalicylic Acid.Essay Analgesics.Experiment 9: Isolation of the Active Ingredient in an Analgesic Drug.Experiment 10: Acetaminophen.Experiment 10A: Acetaminophen (Microscale Procedure).Experiment 10B: Acetaminophen (Semi-Microscale Procedure).Essay Identification of Drugs.Experiment 11: TLC Analysis of Analgesic Drugs.Essay Caffeine.Experiment 12: Isolation of Caffeine from Tea or Coffee.Experiment 12A: Extraction of Caffeine from Tea with Methylene Chloride.Experiment 12B: Extraction of Caffeine from Tea or Coffee Using Solid Phase Extraction (SPE).Essay Esters¡XFlavors and Fragrances.Experiment 13: Isopentyl Acetate (Banana Oil).Experiment 13A: Isopentyl Acetate (Microscale Procedure).Experiment 12B: Isopentyl Acetate (Semi-Microscale Procedure).Essay Terpenes and Phenylpropanoids.Experiment 14: Essential Oils: Extractions of Oil from Cloves by Steam Distillation and Liquid Carbon Dioxide.Experiment 14A: Oil of Cloves (Microscale Procedure).Experiment