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This edited volume presents a modern and accessible overview of Nuclear Magnetic Resonance (NMR) spectroscopy, highlighting its fundamental principles, recent technological advancements, and wide-ranging applications across chemistry and biomolecular science. Designed for researchers, educators, and advanced students, this book explores key techniques used for elucidating molecular structure, dynamics, and interactions. With emphasis on both high-field and benchtop NMR instrumentation, readers will gain insights into emerging analytical strategies, data interpretation methods, and the integration of NMR with computational and AI-based tools. The volume showcases how NMR continues to evolve as a versatile and indispensable tool for structural chemistry, materials analysis, metabolomics, and bioorganic investigations. Embracing innovation while retaining a strong foundation in theory, this book offers a clear and compelling guide for those seeking to expand their expertise or apply NMR in novel research contexts. A valuable resource for both academic and industrial laboratories, the volume bridges traditional knowledge with contemporary approaches, ensuring relevance in today's data-driven scientific landscape.