Like its previous five editions, this book is ideally suited for use in a sophomore-level laboratory course in organic chemistry. This truly comprehensive yet compact lab manual offers a wide range of excellent experiments in a variety of scales - from micro to semi micro. Clear instructions and safety information is also included, as well as recipes for the preparation of organic compounds and procedures for the preparation of compounds with interesting properties. Safety instructions are included throughout.
Like its previous five editions, this book is ideally suited for use in a sophomore-level laboratory course in organic chemistry. This truly comprehensive yet compact lab manual offers a wide range of excellent experiments in a variety of scales - from micro to semi micro. Clear instructions and safety information is also included, as well as recipes for the preparation of organic compounds and procedures for the preparation of compounds with interesting properties. Safety instructions are included throughout.
Safety. Glassware Used in the Organic Chemistry LabCleaning Up. Collection and Disposal of Waste. The Laboratory Notebook. The Chemical Literature. Tables. Filtration. Recrystallization. Distillation. Reduced Pressure Distillation. Distillation of Mixtures of Two Immiscible Liquids: Steam Distillation. Sublimation. Extraction by Solvents. Chromatography. Removal of Water. Boiling Point. Melting Point. Density. Index of Refraction. Optical Activity. Molecular Weight. Solubility. Infrared Absorption Spectrometry. Ultraviolet Visible Absorption Spectrometry. Nuclear Magnetic Resonance Spectrometry. Mass Spectrometry. Qualitative Tests for the Elements. Qualitative Characterization Tests: Tests for Functional Groups. Characterization Through Formation of Derivatives. Assembling the Apparatus. Temperature Control. Methods of Heating and Cooling. Stirring. Addition of Reagents. Control of Evolved Gases. Concentration. Use of an Inert Atmosphere. Working Up the Reaction.
Safety. Glassware Used in the Organic Chemistry LabCleaning Up. Collection and Disposal of Waste. The Laboratory Notebook. The Chemical Literature. Tables. Filtration. Recrystallization. Distillation. Reduced Pressure Distillation. Distillation of Mixtures of Two Immiscible Liquids: Steam Distillation. Sublimation. Extraction by Solvents. Chromatography. Removal of Water. Boiling Point. Melting Point. Density. Index of Refraction. Optical Activity. Molecular Weight. Solubility. Infrared Absorption Spectrometry. Ultraviolet Visible Absorption Spectrometry. Nuclear Magnetic Resonance Spectrometry. Mass Spectrometry. Qualitative Tests for the Elements. Qualitative Characterization Tests: Tests for Functional Groups. Characterization Through Formation of Derivatives. Assembling the Apparatus. Temperature Control. Methods of Heating and Cooling. Stirring. Addition of Reagents. Control of Evolved Gases. Concentration. Use of an Inert Atmosphere. Working Up the Reaction.
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