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Neutron and synchrotron facilities, which are beyond the scale of the laboratory, and supported on a national level in countries throughout the world. These tools for probing micro- and nano-structure research and on fast dynamics research of atomic location in materials have been key in the development of new polymer-based materials. Different from several existing professional books on neutron science, this book focuses on theory, instrumentation, an applications. The book is divided into five parts: Part 1 describes the underlying theory of neutron scattering. Part 2 describes the…mehr
Neutron and synchrotron facilities, which are beyond the scale of the laboratory, and supported on a national level in countries throughout the world. These tools for probing micro- and nano-structure research and on fast dynamics research of atomic location in materials have been key in the development of new polymer-based materials. Different from several existing professional books on neutron science, this book focuses on theory, instrumentation, an applications.
The book is divided into five parts:
Part 1 describes the underlying theory of neutron scattering.
Part 2 describes the various instruments that exist and the various techniques used to achieve neutron scattering or bombardment.
Part 3 discusses data treatment and simulation methods as well as how to assess the environment of the sample (temperature, pressure, shear, and external fields).
Part 4 addresses the myriad applications of small and large molecules, biomolecules, and gels.
Part 5 describes the various global neutron sources that exist and provides an overview of the different reactors.
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Autorenporträt
TOYOKO IMAE, PhD, is a professor at the Graduate Institute of Engineering at National Taiwan University of Science and Technology, Taiwan, working on various aspects of polymers and nanomaterials, and a professor emeritus at Nagoya University, Japan. TOSHIJI KANAYA, PhD, is a professor at the Institute for Chemical Research at Kyoto University in Japan, where he specializes in areas of polymer physics. Professor Kanaya has contributed to the book Polyolefin Composites , also from Wiley. MICHIHIRO FURUSAKA, PhD, is a professor at the Graduate School of Engineering at Hokkaido University, Japan, working in the field of neutron instrumentation and optics. NAOYA TORIKAI, PhD, is an associate professor at the Graduate School of Engineering at Mie University, Japan, working in research areas of polymer physics, after serving as an instrument scientist of a pulsed neutron reflectometer at High Energy Accelerator Research Organization (KEK).
Inhaltsangabe
Preface vii Contributors ix I Neutron Scattering 1 I.1 Basics Concepts 1 Ferenc Mezei II Instrumentation 29 II.1 Small-Angle Neutron Scattering 29 II.1.1 Small-Angle Neutron Scattering at Reactor Sources 29 Kell Mortensen II.1.2 SANS Instruments at Pulsed Neutron Sources 57 Toshiya Otomo II.1.3 Ultra-Small-Angle Neutron Scattering 73 II.1.3.1 Bonse-Hart USANS Instrument 73 Michael Agamalian II.1.3.2 Focusing USANS Instrument 94 Satoshi Koizumi II.2 Neutron Reflectometry 115 Naoya Torikai II.3 Quasielastic and Inelastic Neutron Scattering 147 II.3.1 Neutron Spin Echo Spectroscopy 147 Michael Monkenbusch and Dieter Richter II.3.2 Neutron Backscattering 183 Bernhard Frick and Dan Neumann II.3.3 Time-of-Flight Spectrometry 203 Ruep E. Lechner II.4 Neutron Imaging 269 Nobuyuki Takenaka III Data Treatment and Sample Environment 285 III.1 Practical Aspects of SANS Experiments 285 George D. Wignall III.2 Structure Analysis 311 Hideki Seto III.3 Calculation of Real Space Parameters and Ab Initio Models from Isotropic Elastic SANS Patterns 329 Peter V. Konarev and Dmitri I. Svergun III.4 Contrast Variation 351 Mitsuhiro Hirai III.5 Sample Environment: Soft Matter Sample Environment for Small-Angle Neutron Scattering and Neutron Reflectometry 383 Peter Lindner, Ralf Schweins, and Richard A. Campbell IV Applications 415 IV.1 Hierarchical Structure of Small Molecules 415 Tsang-Lang Lin IV.2 Structure of Dendritic Polymers and Their Films 435 Koji Mitamura and Toyoko Imae IV.3 Dynamics of Polymers 455 Toshiji Kanaya and Barbara J.Gabrys IV.4 Inhomogeneous Structure and Dynamics of Condensed Soft Matter 493 Mitsuhiro Shibayama IV.5 Protein Dynamics Studied by Neutron Incoherent Scattering 517 Mikio Kataoka and Hiroshi Nakagawa IV.6 Polymer Interfaces and Thin Films 539 David G. Bucknall IV.7 Neutron Diffraction from Polymers and Other Soft Matter 571 Geoffrey R. Mitchell V Current Facilities 601 V.1 Pulsed Neutron Sources and Facilities 601 Masatoshi Arai V.2 Reactor Overview 621 Colin J. Carlile Index 643
Preface vii Contributors ix I Neutron Scattering 1 I.1 Basics Concepts 1 Ferenc Mezei II Instrumentation 29 II.1 Small-Angle Neutron Scattering 29 II.1.1 Small-Angle Neutron Scattering at Reactor Sources 29 Kell Mortensen II.1.2 SANS Instruments at Pulsed Neutron Sources 57 Toshiya Otomo II.1.3 Ultra-Small-Angle Neutron Scattering 73 II.1.3.1 Bonse-Hart USANS Instrument 73 Michael Agamalian II.1.3.2 Focusing USANS Instrument 94 Satoshi Koizumi II.2 Neutron Reflectometry 115 Naoya Torikai II.3 Quasielastic and Inelastic Neutron Scattering 147 II.3.1 Neutron Spin Echo Spectroscopy 147 Michael Monkenbusch and Dieter Richter II.3.2 Neutron Backscattering 183 Bernhard Frick and Dan Neumann II.3.3 Time-of-Flight Spectrometry 203 Ruep E. Lechner II.4 Neutron Imaging 269 Nobuyuki Takenaka III Data Treatment and Sample Environment 285 III.1 Practical Aspects of SANS Experiments 285 George D. Wignall III.2 Structure Analysis 311 Hideki Seto III.3 Calculation of Real Space Parameters and Ab Initio Models from Isotropic Elastic SANS Patterns 329 Peter V. Konarev and Dmitri I. Svergun III.4 Contrast Variation 351 Mitsuhiro Hirai III.5 Sample Environment: Soft Matter Sample Environment for Small-Angle Neutron Scattering and Neutron Reflectometry 383 Peter Lindner, Ralf Schweins, and Richard A. Campbell IV Applications 415 IV.1 Hierarchical Structure of Small Molecules 415 Tsang-Lang Lin IV.2 Structure of Dendritic Polymers and Their Films 435 Koji Mitamura and Toyoko Imae IV.3 Dynamics of Polymers 455 Toshiji Kanaya and Barbara J.Gabrys IV.4 Inhomogeneous Structure and Dynamics of Condensed Soft Matter 493 Mitsuhiro Shibayama IV.5 Protein Dynamics Studied by Neutron Incoherent Scattering 517 Mikio Kataoka and Hiroshi Nakagawa IV.6 Polymer Interfaces and Thin Films 539 David G. Bucknall IV.7 Neutron Diffraction from Polymers and Other Soft Matter 571 Geoffrey R. Mitchell V Current Facilities 601 V.1 Pulsed Neutron Sources and Facilities 601 Masatoshi Arai V.2 Reactor Overview 621 Colin J. Carlile Index 643
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